FACILITIES

Mass Spectrometer

Varian Stingray FT-IR Imaging System (IRIRI)

FT-IR Accessories

Nuclear Magnetic Resonance

Fluorescence Spectroscopy

Inspector Raman

Renishaw inVia Raman Microscope

Fourier Transform Infrared Spectroscopy

Ultraviolet-visible (UV-Vis) Spectroscopy

Goniometer and Laser Light Scattering System

Nano Dynamic Light Scattering Dector

Polarized Light Microsocpy

Impedance Analyzers

Ellipsometer

 

Spectroscopic Cluster

 

Bruker Daltronic Microflex
MALDI TOF Mass Spectrometer

 

 


Bruker Daltronic Microflex
MALDI TOF Mass Spectrometer


Contact: Hans Schanz
Department of
Chemistry & BioChemistry

Bruker Daltronic Microflex MALDI TOF Mass Spectrometer

The instrument features a gridless ion reflectron for high mass resolution and accuracy, a PSD (Post Source Decay) system which enables MS/MS capability, and an extensive software package, Biotools 2.2 and PolyTools 1.0, for analysis of polymers, biopolymers, proteins and peptides.

MALDI source

  • microScout Ion Source with state-of-the-art pulsed ion extraction (PIE™)
  • Target area exactly one fourth of industry standard microtiter plates
  • Various 96-spot target types available for specific applications
  • Compatible with Bruker Daltonics sample preparation robotics
  • Nitrogen laser with variable repetition rate up to 20 Hz
  • Patented AnchorChip MALDI target technology for fast automation, increased sequence coverage and 10–100 fold sensitivity increase over stainless steel target holder

TOF Analyzer

  • High resolution reflectron configuration or optional linear only version
  • Optional MS/MS capability with auto PSD (automated post-source decay) including pre-cursor ion selection device

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Varian Stingray FT-IR Imaging System
Biorad Digilab series FTS 6000 Series
FT-IR Spectrometer

 

 



Stingray FT-IR
Imaging System


Contact: Marek Urban
Urban Research Group

Varian, Inc Stingray™ FT-IR Imaging System

The Stingray FT-IR imaging system brings together Varian's premier step-scan FTS 6000 spectrometer, a UMA 600 microscope designed for both single point and imaging, the widest selection of FPA detectors and Resolutions Pro software. This powerful, easy-to use, turnkey system provides a revolutionary solution to capturing, identifying, visualizing and analyzing heterogeneity in both micro and macro sampling applications. Stingray spectrochemical imaging analysis can be applied to a huge range of samples and disciplines, from biology to polymer chemistry, from contamination and failure analysis to new material development.

Features

  • Simultaneous spectral and spatial sampling
  • Highest spatial resolution possible - down to 5 microns
  • Multiple Ranges (Mid and Near IR) and Speeds (Rapid or Step-Scan)
  • Designed for user flexibility:
    • Single-point and multiple array detector sizes available (16 x 16 to 128 x 128)
    • Dual-array systems
  • Multiple sampling options: Micro and Macro capability
  • ATR imaging for difficult-to-analyze samples
  • Large mosaic images to cover the entire sample

Features of the UMA 600 Microscope include Patented view through aperture lets you see exactly the sample under the infrared. The advanced optical design eliminates stray light and the need for redundant aperturing. Samples can be viewed by both binocular and video modes. Infinity corrected, all reflecting optics without the need for dichroics provides the ultimate in detectability and throughput. Dual detector capability equips the microscope with two single point detectors, an array and a single point detector or dual focal plane arrays, to minimize the "down time" of detector changes. Zoom capability in both visible and IR gives the flexibility to use higher magnification if necessary without physically changing the objective. A motorized aperture gives precise control from either the computer or the microscope and enhances the ease of use.Auto focus in both the infrared for sample analysis and in the visible for video camera assures that the picture you see or the data you acquire are optimal. Data collection can be started from the microscope since most operators work from the microscope not the computer. Automated multi point analysis AMPA™ allows unattended analysis of many points on the same samples or many samples on the sample holder. Micro-ATR, Grazing Angle Objective, side-reflection objective and polarizer (IR and visible) options provide measurement solutions for the most difficult samples. Upgrade to infrared spectrochemical imaging (Stingray or FastImageIR).

Includes a Panasonic GP-KR222 1/2" Digital Signal Processing Camera.

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FT-IR Accessories

 

 


Pike MIRacle ATR Micro-ATR

Contact: Marek Urban
Urban Research Group

Pike MIRacle ATR Micro-ATR

Micro-ATR can be used to analyze films, pastes, solids, liquids and powders. Because of the reproducible effective pathlength, it is well suited for both, qualitative and quantitative applications. It has the highest IR throughput and flexibility. It uses a Ge crystal that is easily changed or replaced. There is an optical specular reflectance plate for measurement of coatings on reflective surfaces, and different pressure clamps to suit the sample.

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Axiom Analytical Tunnel
CIR Cell ATR


Contact: Marek Urban
Urban Research Group


Axiom Analytical Tunnel CIR Cell ATR

Axiom Tunnel Cells are the first attenuated total reflectance (ATR) devices to provide both the high degree analytical accuracy and the reliability required for a variety of demanding analyses. As a result, these devices are helping to create new opportunities for FTIR spectroscopy in application areas ranging from HPLC detection to process methods development and even the instrumentation of large process reactions. The proprietary Tunnel* optical design provides performance far superior to other cylindrical internal reflectance (CIR) cells. When combined with adjustment-free construction, this optical design results in significantly enhanced absorption, high transmission, and unmatched linearity and repeatability. These features make the Tunnel Cell ideal for the most rigorous applications whether in the lab or on the process line.

These Tunnel Cells feature sample volumes ranging from 40 microliters to 75 milliliters - and can be operated at pressures to over 1200 psi. Most models employ a helical flow geometry which eliminates dead volume and maximizes cleaning efficiency. Even highly viscous samples can be analyzed and then rapidly flushed out with no measurable sample retention.

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Pike EasiDiff
Diffuse Reflectance


Contact: Marek Urban
Urban Research Group


Pike EasiDiff Diffuse Reflectance

This technique offers an efficient way of collecting spectra of powders and other solid materials. Although sample preparation involves its grinding with KBr, no pellet pressing is required. The powder it is simply placed into the sample cup and analyzed. Among others, diffuse reflectance accessories are ideal for pharmaceutical and forensic applications. Automated versions speed analysis.

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Pike Classic VATR
Variable-angle ATR


Contact: Marek Urban
Urban Research Group


Pike Classic VATR Variable-angle ATR

This is an in-compartment accessory with the ATR crystal mounted vertically with respect to the spectrometer base plate. Its optical layout is based on an optimized Gilby configuration and allows continuous adjustment of the incident beam angle between 30 and 60 degrees. This is suitable for the analysis of solids, films, and coatings. You have full control over the number of reflections and depth of penetration. It has a unique mechanism for fine-tuning mirror positions and precise and repeatable alignment, and high energy thoughput. We have both KRS-5 and Ge crystals, for a larger range of depth profiling.

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Harrick GATR IR attachment

Contact: Marek Urban
Urban Research Group


Harrick GATR IR attachment

The GATR™ is a revolutionary accessory using 65° grazing angle ATR for studies of adsorbed species and monolayers on substrates. Harrick's GATR™ is the most sensitive method available for examining extremely thin coatings on semiconductors and metals by FTIR spectroscopy.

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MTEC Photoacoustic

Contact: Marek Urban
Urban Research Group


MTEC Photoacoustic

FTIR photoacoustic spectroscopy has capabilities for both depth profiling and spectral range. FTIR/PAS performance levels for depth-profiling have also improved due to the introduction of step-scan FTIR spectrometers. This allows both the magnitude and phase of the photoacoustic signal to be easily analyzed. This facilitates elucidation of depth dependent molecular information due to gradient or layered compositions. FTIR/PAS data can be plotted s o that the relative depths of absorption can be identified for specific infrared absorbance bands. This aids in determining the ordering of layers in layered materials on a micron dimensional scale which is not accessible with an infrared microscope. These scanning capabilities combined with advances in signal processing allow sensing depth to be varied from less than a micrometer to over 100 micrometers in polymers. The expanded mirror velocity range of the new generation of research grade spectrometers also opens the door to measurements from the ultraviolet through the far infrared spectral regions. This is especially advantageous for PAS measurements because the technique's minimal sample preparation requirement and nondestructive capability have always made it applicable in many areas of chemical and biological research.

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Pike 80 Spec Grazing Angle
Specular Reflectance for
Relatively Thin Films


Contact: Marek Urban
Urban Research Group


Pike 80 Spec Grazing Angle Specular Reflectance

for Relatively Thin Films

Ideal for the measurement of relatively thin films and mono-molecular layers by specular reflectance. Available to use polarized light both incoming and outgoing. It includes gold coated reflective optics for highest throughput grazing angle analysis, dual polarizer mounts for incoming and outgoing IR beam, optional samples masks version to define unique sampling areas, and a baseplate mount design for stable operation and collection of high quality spectra.

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Nuclear Magnetic Resonance

 

 


Varian Inova 500 MHz
NMR Spectrometer


Contact: Bill Jarrett

Varian Inova 500 MHz NMR Spectrometer

  • 3-channel system, 2 full band 1 low band, 2 channels with waveform generators
  • Magnet equipped with vibration isolators
  • FTS cooling system for extend -5oC operation
  • VT controller
  • Performa III gradient
  • 2 probes
  • 2-channel 5mm standard broadband PFG probe
  • 3-channel 5mm PFG inverse probe
  • SUN ULTRA 10 workstation

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Varian Inova 400 MHz
NMR Spectrometer


Contact: Bill Jarrett


Varian Inova 400 MHz NMR Spectrometer

  • 3-channel system, 2 full band, 1 low band, and 2 channels with waveform generators
  • 3 KW amplifiers (2 AMT models, Chemagnetics 1H amplifier)
  • VT controller
  • MAS controller
  • 2 probes
  • 2-channel 7.5 mm broadband Chemagnetics CP/MAS probe, VT range -100°C to 250°C
  • 3-channel 4mm HXY Chemagnetics REDOR probe, VT range -100°C to 250°C
  • SUN ULTRA 5 workstation

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Varian Mercury 300 MHz
NMR Spectrometer


Contact: Bill Jarrett


Varian Mercury 300 MHz NMR Spectrometer

  • 2-channel 4 nuclei system (1H, 13C, 19F, 31P)
  • Performa I gradient
  • 2-channel 5mm standard broadband PFG probe
  • VT controller

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Varian Mercury 200 MHz
NMR Spectrometer


Contact: Bill Jarrett


Varian Mercury 200 MHz NMR Spectrometer

Nuclear Magnetic Resonance (NMR) spectroscopy allows a user to characterize a sample gaining morphological and compositional knowledge. The Varian MERCURY 200 is equipped to run RT, 1H and 13C spectra Includes a 2-channel 4 nuclei system (1H, 13C, 19F, 31P) and a 2-channel 5mm standard broadband probe with a VT controller.

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Fluorescence Spectroscopy

 

 


Zeiss LSM 510 META

Contact: Sabine Heinhorst
Department of Chemistry

Zeiss LSM 510 META

In the way it implements the confocal principle, the design of the unmatched. It allows multi fluorescence images to be collected without compromising resolution and efficiency.

Imagine the new Unprecedented flexibility for individual applications. Innovative acquisition and processing functions that guarantee fast and efficient structural and functional analysis of your specimens. A stable and reliable system, allowing you to concentrate on the content of your research. A system that lays the foundations for your future success - the LSM 510 META.

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TECAN Safire²™ Fluorescence Spectrometer


Contact: Robert Lochhead


TECAN Safire²™ Fluorescence Spectrometer

In Safire² has been developed with the drug discovery process in mind. Due to its in-built flexibility, sensitivity and performance, Safire² is the ideal instrument to bridge the gap between assay development and high throughput screening. Safire² is a fully modular microplate detection system based on the quad-4 monochromator technology that offers a range of high speed detection techniques. In assay development and demanding research environments, where frequent changing of applications and fluorophores is required, Safire² eliminates the need for cumbersome filter changes thereby saving time and money. The modular concept of Safire² allows upgrades to new detection modes at any time if there is a need to have access to further applications. Detection modules are available for

 top and bottom fluorescence intensity measurements, fluorescence polarization studies and multi-channel absorbance and luminescence measurements. Safire² is easily combined with a stacker module for batch processing of up to 50 microplates.

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Inspector Raman™

 

 


Inspector Raman™

Contact: Marek Urban
Urban Research Group

DeltaNu Inspector Raman™

The Inspector Raman™ is a robust, portable Raman spectrometer that fits in your hand for analysis of solids, liquids, pastes, and slurries. This lightweight, dispersive spectrometer has no moving parts and may be used in any position. Raman spectroscopy offers the advantage of identifying various substances by their unique fingerprint, based on the chemical structure of the unknown, and can do so through walls of sealed bags, transparent bottles, flasks, vials, and ampoules without opening the container. Data is retrieved remotely with Blue Tooth technology or USB with a Fujitsu laptop and NuSpec™ software. Spectral libraries are developed using DeltaNus library development software for identification of unknown substances and quantification of various compounds.

Applications

  • Reaction monitoring
  • Authentication of historical works of art
  • Raw material identification
  • Analysis of organometallic compounds in a glove box
  • Botanical research
  • Octane number in fuels
  • Edible oil analysis

Features and Specifications

  • Solids: Point and shoot attachment
  • Liquids: Sample cell attachment for 8mm vials, NMR tubes, or MP tubes
  • Microscopy: Optional microscope attachment (NuScope™)
  • Portability
    • weighs under 5 lbs
    • remote trigger
    • wireless Blue Tooth connectivity (or USB)
    • battery powered with 5 hours of continuous use
  • Instrument specifications:
    • laser: 70mW 785 nm
    • resolution: 10 cm-1
    • spectral range: 250 cm-1 – 2000 cm-1

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Renishaw inVia Raman Microscope

 

 


Renishaw inVia Raman Microscope

Contact: Marek Urban
Urban Research Group

Renishaw inVia Raman Microscope

Renishaw's inVia Raman microscopes are high-performance Raman instruments with simplicity of operation and unparalleled flexibility. inVia Raman microscopes are high sensitivity systems with integrated research grade microscopes, enabling high resolution confocal measurements. inVia Raman microscopes support multiple lasers, with automatic software switching of excitation wavelength and provide full optical path optimisation. Exceptional sensitivity comes as standard in all inVia Raman microscopes, offering ultra-low signal detection with minimum noise. This inVia system has Renishaw's powerful WiRE™ 2.0 software for intuitive operation and data manipulation, Renishaw's high sensitivity ultra-low noise RenCam CCD detector, and Renishaw's high stability honeycomb baseplate with precision kinematic mounts for easy laser swapping.

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Fourier Transform Infrared Spectroscopy


Bruker TENSOR™ 37 FTIR

Contact: Robert Lochhead

Bruker TENSOR™ 37 FTIR

With the new DigiTect™ detector system, TENSOR™ provides highest sensitivity performance. Permanently aligned, high throughput RockSolid™ interferometer ensures stability and durability. Online PerformanceGuard™ is the insurance for accurate results. All optical components, automation units and accessories of TENSOR™ are monitored continuously. The TENSOR™ series are equipped with automatic accessory and automatic component recognition systems. When an accessory is placed in the sample compartment the accessory will be instantly and automatically recognized and tested. All relevant parameters transferred to the software, so that you can immediately start your measurements. All optical components like source, detector, beamsplitter, and laser can easily be changed and are recognized by the IntelliSense™ coding. It is possible to expand the wavelength range to NIR (TENSOR™ 37). TENSOR™ Series utilizes a large sampling compartment and can house a 96 well plate, it is equipped with an HTS-XT microtiter plate extension.

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Biorad Digilab Series 7000
FT-IR Spectrometer


Contact: Marek Urban
Urban Research Group


Biorad Digilab Series 7000 FT-IR Spectrometer

The FTS 7000 Series FTIR spectrometers offer the highest optical performance and the most advanced software to solve your toughest challenges. Powered by a high wattage water-cooled infrared source, the FTS 7000 spectrometers have at their core a frictionless air-bearing interferometer, which simultaneously maximizes the spectral throughput and minimizes the noise in their measurements.

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Bruker Equinox 55
FT-IR Spectrometer


Contact:
Kenneth Mauritz
Robson Storey

Mauritz Research Group
Storey Research Group


Bruker Equinox 55 FT-IR Spectrometer

EQUINOXT stands for equivalent inputoutput exchange and refers to the innovative port design on the EQUINOX 55. Four of the six output ports have dual functionality - these ports can be used as input or output ports and selection of the configuration is done via the software. For example, the FT-Raman accessory can be mounted on the right hand side, an IR microscope at the front, a near-IR fiber optic coupling unit at the back, and an external sample compartment on the left. Bruker Optics' unique EQUINOXT concept results in the highest experimental versatility of any FT-IR spectrometer available. Equivalency between the source and detector positions means that a transmission spectrum and an emission spectrum can be obtained from a single sample in the sample compartment. Output ports are available on all four sides of the spectrometer allowing to four external accessories to be mounted simultaneously. The EQUINOX 55 offers the highest experimental versatility available in an FT-IR spectrometer.

The standard spectral resolution of better than 0.5 cm-1 is suitable for most applications. However, should the application change, resolution capabilities can be upgraded to 0.16 cm-1 . Fast rapid scan, step scan and "slow scan" are available for a variety of demanding applications. In its base configuration, the EQUINOX 55 covers a wide range in the mid- and near-IR regions. Range extension packages are available to enable high sensivity measurements from the visible to 30 cm-1 .

The EQUINOX 55 offers several options for changing beamsplitters. Full automatic operation is provided with Bruker Optics' sealed beamsplitter enclosure. This unique beamsplitter housing locks into the interferometer cover and the beamsplitter is changed via push button control, without breaking the optics seal. Manual beamsplitter change is also offered for those who prefer the direct approach. No scanner realignment is required after beamsplitter replacement making range change a breeze.

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Digilab Scimitar FTS 2000
Series FT-IR Spectrometer


Contact: Marek Urban
Urban Research Group


Digilab Scimitar FTS 2000 Series FT-IR Spectrometer

The system is designed with a simple USB computer interface, advanced diagnostics, and validation and certification protocols. Includes the new Resolutions. spectral analysis software, new validation and diagnostics packages and Digilab's traditionally high throughput and S/N.

Features include:

  • PermaTrac 3™ interferometer
  • Patented AutoTrac™ dynamic alignment
  • Patented DuraGlow™ Source Resolutions.
  • Available upgrade to Resolutions Pro™ Software
  • KBr and Quartz beamsplitter
  • Mid-IR and NIR configuration
  • Cooled DTGS, PbSE or InGaAs detector
  • 0.5 cm-1 resolution
  • Pentium based computer

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Digilab Scimitar FTS-2000
UMA 400 IR Microscope


Contact: Thames-Rawlins
Research Group


Digilab Scimitar FTS-2000

UMA 400 IR Microscope

The Scimitar family of FT-IR spectrometers includes a patent-pending high-energy Duraglow™ source that is the brightest, most stable and longest lasting air-cooled source. With the new Permalign™ interferometer and Digilab's high throughput optics, the Scimitar offers performance never available at this price. Using patented technologies derived from our research spectrometers, the Scimitar family offers a wide variety of upgrades including FTIR microscopy. The system is designed with a simple USB computer interface, advanced diagnostics, and validation and certification protocols. Available in mid-IR and near-IR configurations, these systems provide ease-of-use enabling you to solve your spectroscopic problems. Features include PermaTrac 3™ interferometer, Patented AutoTracAutodynamic alignment, Patented DuraGlow™ Source, Resolutions Software, KBr and Quartz beamsplitter, Mid-IR and NIR configuration, Cooled DTGS, PbSE or InGaAs detector, 0.5 cm-1 resolution, and a Pentium based computer. Applications include general purpose educational instrument, routine quality control, routine spectral verification, ATR analysis, DRIFTS Analysis, routine Hyphenated Techniques: GC-IR and TGA-IR Microscopy. Capabilities include Variable Angle ATR, Slide-on micro ATR analyzer, Diffuse reflectance, and Hot Stage.

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Bruker IFS 88
with Oriel Lamp System


Contact: Charles Hoyle
Hoyle Research Group


Bruker IFS 88 with Oriel Lamp System

Infrared spectroscopy (IR) probes the characteristic vibrational and rotational energy for various functional groups present within a molecule. RTIR spectroscopy also serves as a tool for in-situ real time monitoring of chemical and physical changes during processing of reactive materials such as polymerizations and reactions induced thermally and photochemically Scanning rate is an approximately 15 scan/sec. The instrument is a Bruker IFS 88 with an Oriel lamp system.

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Ultraviolet-visible (UV-Vis) Spectroscopy

 

 


Cary 500 Scan UV-Vis
Spectrometer


Contact: Charles Hoyle
Hoyle Research Group

Cary 500 Scan UV-Vis Spectrometer

UV-Vis spectroscopy (uv = 200-400 nm, visible = 400-800 nm) probes the electronic transitions of molecules as they absorb light in the UV and visible regions of the electromagnetic spectrum. We use the instrument to examine the absorbance spectrum of photoinitiators, molecules which start a reaction upon the absorption of light.

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Beckman DU640
UV Spectrometer


Contact: Sergei Nazarenko
Sergei Nazarenko's Page

Beckman DU640 UV Spectrometer

This is the full featured scanning UV/Vis spectrophotometer with a stable beam optical design with an extended wavelength range from 190 to 1100 nm and bandpass of 1.8 nm. Beckman DU640 is a full featured scanning UV-VIS-NIR spectrophotometer with a stable beam optical design, extended wavelength range from 190-1100nm, and bandpass of 1.8nm, 6-cell high-performance transport, Software version N, applications include Protein, Nucleic Acid, Enzyme Mechanism, and DNA/Oligo Quant. This is a great spec with an internal computer. Manufactured in 1997, dimensions are 27x21x11in.

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Polarized Light Microscopy (PLM)

 

 


Polarized Light
Microscopy (PLM)

Contact: Kenneth Mauritz
Mauritz Research Group

Polarized Light Microscopy (PLM)

PLM is a tool to aid in studies of crystallization kinetics and morphology. Equipped with a Mettler® hot stage and Nikon® digital camera and software, we are able to take high resolution micrographs and measure spherulite size or spherelite banding periodicity, as well as spherulitic growth rates.

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Impedance Analyzers

 

 


HP 4192A LF Impedance Analyzer

Contact: Kenneth Mauritz
Mauritz Research Group

HP 4192A LF Impedance Analyzer

  • 5 Hz to 13 MHz variable frequency
  • Swept Measurement Capability
  • Gain-phase measurements: amplitude, phase, group delay
  • Floating or grounded devices
  • Impedance measurement: |Z|, |Y|, Theta, R, X, G, B, L,
  • C, D, Q, Delta, Delta%
  • GPIB

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Solartron Impedance
Analyzer


Contact: Kenneth Mauritz
Mauritz Research Group


Solartron Impedance Analyzer

Using dielectric spectroscopy and impedance analysis we are able to evaluate the effects of morphological control on transport properties, such as proton conductivity in perfluorinated ionomers.

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Gaertner Ellipsometer 7109

 

 



Gaertner Ellipsometer 7109

Contact: Sergei Nazarenko
Sergei Nazarenko's Page


Gaertner Ellipsometer 7109

This is the full featured scanning UV/Vis spectrophotometer with a stable beam optical design with an extended wavelength range from 190 to 1100 nm and bandpass of 1.8 nm. Beckman DU640 is a full featured scanning UV-VIS-NIR spectrophotometer with a stable beam optical design, extended wavelength range from 190-1100nm, and bandpass of 1.8nm, 6-cell high-performance transport, Software version N, applications include Protein, Nucleic Acid, Enzyme Mechanism, and DNA/Oligo Quant. This is a great spec with an internal computer. Manufactured in 1997, dimensions are 27x21x11in.

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